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یافته ها: ترکیب شماره یک: ترکیبی فلاونوئیدی شناسایی شده از زیر فراکسیون Fr.d1.3 [pic] بررسی طیف 1H-NMR : 1H-NMR (CDCI3): δ ppm: 12.62 (s, 1H, OH-5), 8.07 (d, J=8.9Hz, 2H', H-6'), 6.87 (d, J=8.9 Hz, 2H, H-3', H-5'), 6.43 (d, J=2.0 Hz, 1H, H-8), 6.19 (d, J=2Hz, 1H, H-6), 5.33 (d, J=5.1Hz, 1H, H-1''), 3.76- 3.17(m, 5H of arabinose H2O). طیف 13C-NMR : 13CNMR (CDCl3) δ ppm: 177.58 (C-4), 164.29 (C-7), 161.24(C-5), 160.09 (C-4'), 156.38 (C-9), 156.25 (C-2), 133.58 (C-3), 131.03 (C-2', 6'), 120.71 (C-1'), 115.32 (C-3',5'), 103.97 (C-10), 101.25 (C-1''), 98.76 (C-6), 93.73 (C-8), 71.60 (C-2''), 70.82(C-3''), 66.06 (C-4''), 64.26 (C-5''). ترکیب شماره دو: ترکیب آلکالوئیدی از خانواده بیسانولید آسریدین شناسایی شده از زیر فراکسیون Fr.4.1 [pic] بررسی طیف 1H-NMR : 1H-NMR (DMSO): δ ppm: 8.24 (s, H-6), 7.65(dd, J= 6.3, 8.0Hz, H-2), 7.97 (d, J=6.3, H-4), 7.22 (t, J=6.3, H-3), 7.78 (d, J=8.0, H-1), 7.53 (s, H-5), 4.96 (d, J=2, H-11), 5.50 (d, J=2.0, H-12), 3.35 (s, H-14). طیف 13C-NMR : 13C-NMR (DMSO): δ ppm: 166.4 (C-9), 141.1 (C-6), 149.4 (C-8), 143.2 (C-7'), 141.0 (C-13'), 128 (C-4''), 135.6 (C-2), 128.4 (C-12''), 124.7 (C-4), 121.6 (C-12'''), 123.1 (C-3), 117.6 (C-1), 113.7 (C-4'), 107.4 (C-5), 112.8 (C-8'), 110.3 (C-12'), 90.1 (C-11), 67.7 (C-12), 35.0 (C-14) ترکیب شماره سه : یک آلکالوئید از خانواده آسریدین شناسایی شده از زیر فراکسیون Fr.d1.3 [pic] بررسی طیف 1H-NMR : 1H-NMR (CDCL3): δ ppm: 8.61 (d, J= 4.8Hz, H-6), 7.36 (dd, J= 8.0, 15.0Hz, H-2), 7.99 (d, J=8.0 H-4), 6.96 (t, J=8.0Hz, H-3), 7.33 (d, J=8.0Hz, H-1), 7.66 (d, J=4.8Hz, H-5), 5.09 (d, J=2.7Hz, H-11), 5.26 (d, J=2.7 Hz, H-12), 3.43 (s, H-15), 3.31 (s, H-16), 3.23(s, H-14), 12.89 (s, OH), 9.66 (s, NH). طیف 13C-NMR : 13C-NMR (CDCL3): δ ppm: 168.1 (C-9), 151.3 (C-6), 149.7 (C-8), 140.8 (C-7'), 140.2 (C-13'), 139.4 (C-4''), 1325.0 (C-2), 128.8 (C-12''), 124.0 (C-4), 121.5 (C-12'''), 120.6 (C-3), 116.0 (C-1), 115.0 (C-4'), 110.4 (C-5), 107.8 (C-8'), 104.4 (C-12'), 89.6 (C-11), 76.6 (C-12), 56.3 (C-15), 54.9 (C-16), 35.2 (C-14). شناسایی ترکیب چهار: ترکیب فلاونوئیدی شناسایی شده از زیر فراکسیون Fr.d.5.1.1 [pic] بررسی طیف 1H-NMR : 1H-NMR (DMSO), δ ppm: 12.57 (s, 1H, OH-5), 7.98 (d, J=8.7 Hz, 2H, H-2', 6'), 7.36 (d, H=8.7Hz, 2H, H-2''', 6'''), 7.33(d, J=16 Hz, 1H, H-7'''), 6.85 (d, J=8.7 Hz, 2H, H-3''', 5'''), 6.38(d, J=2.0 Hz, 1H, H-8), 6.14(d, J=2Hz, 1H, H-6), 6.10(d, J=15.9 Hz, 1H, H-8'''), 5.44(d, J=7.5Hz, 1H, H-1''). طیف 13C-NMR : 13C-NMR (DMSO) δ ppm: 177.43(C-4), 166.20(C-9'''), 164.19 (C-7), 161.17 (C-5), 160.01 (C-4'), 159.81(C-4'''), 156.46 (C-2), 156.38 (C-9), 144.62 (C-7'''), 133.07 (C-3), 130.85 (C-2',6'), 130.18(C-2''',6'''), 124.94(C-1'''), 129.79 (C-1'), 115.78 (C-3''', 5'''), 115.11(C-3', 5'), 113.65 (C-8'''), 103.89(C-10), 100.97 (C-1''), 98.79 (C-6), 93.69 (C-8), 76.23 (C-3''), 74.25 (C-2'''), 74.14 (C-5'''), 69.98 (C-4''), 62.98 (C-6''). ترکیب شماره پنج: ترکیب فلاونوئیدی شناسایی شده از زیر فراکسیون Fr.d.5.1.2 [pic] طیف 1H-NMR : Aglycone: 1H NMR (CD3OD) δ ppm: 7.40 (1H, dd, J = 8.3 Hz, H-6), 7.39 (1H, d, J = 2.3, H-2 ), 6.90 (1H, d, J = 8.3 Hz, H-5 ), 6.78 (1H, d, J = 2.2 Hz, H-8), 6.59 (1H, s, H-3), 6.49 (1H, d, J = 2.2 Hz, H-6). beta-Glucopyranoside moiety: δ ppm: 5.06 (1H, d, J = 7.5 Hz, H-1''), 3.94 (1H, dd, J = 2.3, 12 Hz, H-6a''), 3.73 (1H, dd, J = 5.8, 12 Hz, H-6b''), 3.54 (1H, m, J = 9.7, 2.3, 5.8 Hz, H-5''), 3.50 (1H, m, J = 7.5, 9.5 Hz, H-2''), 3.50 (1H, m, J = 9.5, 9,0 Hz, H-3''), 3.41 (1H, t, J = 9.0, 9.7 Hz, H-4''). طیف 13C-NMR : 13C NMR (DMSO-d6): δ ppm: 60.8 (C-6″), 69.7 (C-4″), 73.2 (C-2″), 76.5 (C-3″), 77.3 (C-5″), 94.9 (C-8), 99.7 (C-6), 100.1 (C-1″), 103.3 (C-3), 105.5 (C-10), 113.6 (C-2′), 116.1 (C-5′), 119.4 (C-6′), 121.5 (C-1′), 145.9 (C-3′), 150.1 (C-4′), 157.1 (C-9), 161.2 (C-5), 163.1 (C-7), 164.6 (C-2), 182.1 (C-4).